By Harry ed. Sobotka

ISBN-10: 0120103044

ISBN-13: 9780120103041

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Extra resources for Advances in Clinical Chemistry, Vol. 4

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The Quantitative Spectral Analysis of the Elements,” Vol. 1. G. Fischer, Jena, 1929. L2. , “The Quantitative Spectral Analysis of the Elements,” Vol. 2. G. Fischer, Jena, 1934. , The flame-spectrophotometric determination of calcium in biological fluids and an isotopic analysis of the errors in the Kramer-Tisdall procedure. Biochem. J . 67, 164-172 ( 1957). M2. , Bibliography on analytical flame spectroscopy, Part I. Appl. Spectroscopy 10, 51-64 ( 1956). M3. ” Masson, Paris, 1954. Rl. Russell, B.

Use of the latter on a routine basis has been the cause of confusion and missed diagnoses in patients with nonglucose melliturias. This can have serious consequences in patients with galactosemia and some of the types of melliturias described below. The finding of a urine which has a positive Benedict reaction, but a negative glucose oxidase reaction, is the simplest screening method for the detection of nonglucose melliturias. 2. PRESERVATION Urine specimens which are collected for identification and quantitation of the sugar(s) present can be adequately preserved by adding toluene to the container (4-5 ml for a 24-hour collection) and keeping the urine cool until processed.

Mixed Salt Solution B, 50 mM KC1,5mM K2S04,50 mM NaCl, 150 mM KHZPO?. Calcium Stock Solution, 25 mM CaC12. This is prepared from “Specpure” calcium carbonate in appropriate amount by dissolution in HCl. Perchloric Acid, HC104, 60% (w/w ). Hydrochloric Acid, HCl (sp. gr. 18). Phosphoric Acid, H3POc (sp. gr. 75). 4 mM KH2P04. Sodium Solutions, 200 mM NaC1; 14 mM NaC1. Magnesium Standards for Plasma, Urine, and Feces. Solutions are prepared by adding 10 ml mixed salt solution A, 10 ml calcium solution, and an appropriate volume of magnesium solution I to 700 ml water in a liter flask.

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Advances in Clinical Chemistry, Vol. 4 by Harry ed. Sobotka


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